ChemicalBook CAS DataBase List Bis(4-bromophenyl)phosphine Oxide

Bis(4-bromophenyl)phosphine Oxide synthesis

4synthesis methods

Product Name:Bis(4-bromophenyl)phosphine Oxide
CAS Number:15754-53-7
Molecular formula:C12H9Br2OP
Molecular Weight:359.98

106-37-6 Synthesis

106-37-6
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15754-53-7
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Yield:15754-53-7 73%

Reaction Conditions:

Stage #1: 1.4-dibromobenzenewith magnesium in tetrahydrofuran at 60; for 2 h;
Stage #2: with Diethyl phosphonate in tetrahydrofuran at 25; for 2 h;

References:

Wang, Yang;Lu, Yaoming;Gao, Baoxiang;Wang, Shumeng;Ding, Junqiao;Wang, Lixiang;Jing, Xiabin;Wang, Fosong [Chemical Communications,2016,vol. 52,# 77,p. 11508 - 11511] Location in patent:supporting information

589-87-7 Synthesis

589-87-7
528 suppliers
$10.00/1g

15754-53-7
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References

18620-02-5 Synthesis

18620-02-5
15 suppliers
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15754-53-7
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References

Phosphinous amide, P,P-bis(4-bromophenyl)-N,N-diethyl-

13792-89-7
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15754-53-7
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References