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ChemicalBook CAS DataBase List BIS(4-CHLOROPHENYLTHIO)METHANE

BIS(4-CHLOROPHENYLTHIO)METHANE synthesis

11synthesis methods
-

Yield:2393-97-7 92%

Reaction Conditions:

Stage #1: 3-Bromothiophenolwith sodium hydroxide in ethanol at 80; for 1 h;Inert atmosphere;
Stage #2: diiodomethane in ethanol at 80; for 1 h;Inert atmosphere;

References:

Sankar, Ulaganathan;Mahalakshmi, Susarla;Balasubramanian, Kalapattukuppuswamy [Synlett,2013,vol. 24,# 12,art. no. ST-2013-B0354-L,p. 1533 - 1540] Location in patent:supporting information