ChemicalBook CAS DataBase List (BIS-TERT-BUTOXYCARBONYLMETHYL-AMINO)-ACETIC ACID

(BIS-TERT-BUTOXYCARBONYLMETHYL-AMINO)-ACETIC ACID synthesis

3synthesis methods

Product Name:(BIS-TERT-BUTOXYCARBONYLMETHYL-AMINO)-ACETIC ACID
CAS Number:171557-31-6
Molecular formula:C14H25NO6
Molecular Weight:303.35

Glycine, N,N-bis[2-(1,1-dimethylethoxy)-2-oxoethyl]-, phenylmethyl ester

171557-57-6
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(BIS-TERT-BUTOXYCARBONYLMETHYL-AMINO)-ACETIC ACID

171557-31-6
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$13.00/250mg

Yield:171557-31-6 97%

Reaction Conditions:

with palladium 10% on activated carbon;hydrogen in methanol at 20; for 2 h;

Steps:

Synthesis of 12

Compound 11 (477 mg, 1.17 mmol) was used as a starting material. By the same synthetic procedure as that for 9, 12 (335 mg, 97%) was obtained as a pale yellow oil.

References:

Takahira, Ikuko;Fuchida, Hirokazu;Tabata, Shigekazu;Shindo, Naoya;Uchinomiya, Shohei;Hamachi, Itaru;Ojida, Akio [Bioorganic and Medicinal Chemistry Letters,2014,vol. 24,# 13,p. 2855 - 2858] Location in patent:supporting information

49827-15-8
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$75.00/1g

171557-31-6
57 suppliers
$13.00/250mg

References

5292-43-3 Synthesis

5292-43-3
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171557-31-6
57 suppliers
$13.00/250mg

References