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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
ChemicalBook CAS DataBase List BIS(TRIMETHYLSILYL)CHLOROMETHANE

BIS(TRIMETHYLSILYL)CHLOROMETHANE synthesis

9synthesis methods
a convenient one-pot procedure has been developed by Kemp and Cowley in which trimethylsilylchloride reacts with dichloromethane in the presence of nBuLi at ?110°Cto give bis(trimethylsilyl)dichloromethane.1 This intermediate is sequentially treated with nBuLi and ethanol to yield chlorobis(trimethylsilyl)methane. A number of other syntheses have been described
Chlorotrimethylsilane

75-77-4
564 suppliers
$5.04/10

67-66-3 Synthesis
Chloroform

67-66-3
6 suppliers
$33.60/500ml

(DICHLOROMETHYL)TRIMETHYLSILANE

5926-38-5
44 suppliers
$79.40/5ml

BIS(TRIMETHYLSILYL)CHLOROMETHANE

5926-35-2
35 suppliers
$119.00/5g

BIS(TRIMETHYLSILYL)DICHLOROMETHANE

15951-41-4
16 suppliers
$134.40/1G

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Yield:5926-35-2 3% ，15951-41-4 3% ，5926-38-5 94%

Reaction Conditions:

with N,N,N,N-tetraethylammonium tetrafluoroborate in N,N-dimethyl-formamide; for 29.25 h;electroreduction, anode: Zn, cathode: stainless steel;

References:

Pons, P.;Biran, C.;Bordeau, M.;Dunogues, J. [Journal of Organometallic Chemistry,1988,vol. 358,p. 31 - 38]

BIS(TRIMETHYLSILYL)DICHLOROMETHANE

15951-41-4
16 suppliers
$134.40/1G

BIS(TRIMETHYLSILYL)CHLOROMETHANE

5926-35-2
35 suppliers
$119.00/5g

Lithium, [bis(trimethylsilyl)methyl]-

41823-71-6
0 suppliers
inquiry

Lithium, [chlorobis(trimethylsilyl)methyl]-

27483-93-8
0 suppliers
inquiry

References
Chlorotrimethylsilane

75-77-4
564 suppliers
$5.04/10

Chloromethyltrimethylsilane

2344-80-1
289 suppliers
$15.00/1g

BIS(TRIMETHYLSILYL)CHLOROMETHANE

5926-35-2
35 suppliers
$119.00/5g

References
BIS(TRIMETHYLSILYL)DICHLOROMETHANE

15951-41-4
16 suppliers
$134.40/1G

BIS(TRIMETHYLSILYL)CHLOROMETHANE

5926-35-2
35 suppliers
$119.00/5g

References
Chlorotrimethylsilane

75-77-4
564 suppliers
$5.04/10

67-66-3 Synthesis
Chloroform

67-66-3
6 suppliers
$33.60/500ml

2117-28-4 Synthesis
Bis(trimethylsilyl)methane

2117-28-4
111 suppliers
$37.39/1g

BIS(TRIMETHYLSILYL)CHLOROMETHANE

5926-35-2
35 suppliers
$119.00/5g

TRIS(TRIMETHYLSILYL)METHANE

1068-69-5
60 suppliers
$45.00/50mg

References

BIS(TRIMETHYLSILYL)CHLOROMETHANE Related Search:

1,3-DISILAPROPANE 1,3-DISILABUTANE Bis(trimethylsilyl)methane