ChemicalBook CAS DataBase List Boc-L-Cyclobutylglycine

Boc-L-Cyclobutylglycine synthesis

3synthesis methods

Product Name:Boc-L-Cyclobutylglycine
CAS Number:155905-77-4
Molecular formula:C11H19NO4
Molecular Weight:229.27

(2R)-2-BOC-AMINO-3-PHENYLSULFONYL-1-(2-TETRAHYDROPYRANYLOXY)PROPANE, 98

116611-45-1
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155905-77-4
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$53.00/25mg

Yield:-

Steps:

Multi-step reaction with 5 steps
1: 1) n-BuLi / 1) THF, -78 deg C, 15 min, 2) THF, -78 to -10 deg C
2: n-BuLi / tetrahydrofuran / -40 °C
3: 6percent Na-Hg, Na₂HPO₄ / methanol / 3 h / 0 - 20 °C
4: PPTS / ethanol / 6 h / 50 °C
5: CrO₃, H₂SO₄ / 1 h / 0 - 20 °C

References:

Pauly, Regine;Sasaki, N. Andre;Potier, Pierre [Tetrahedron Letters,1994,vol. 35,# 2,p. 237 - 240]

Carbamic acid, [1-[1-(phenylsulfonyl)cyclobutyl]-2-[(tetrahydro-2H-pyran-2-yl)oxy]ethyl]-, 1,1-dimethylethyl ester, (1R)- (9CI)

155905-73-0
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155905-77-4
79 suppliers
$53.00/25mg

References

116611-45-1
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109-70-6 Synthesis

109-70-6
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155905-77-4
79 suppliers
$53.00/25mg

References

Boc-L-Cyclobutylglycine Related Search:

Nitrilotriacetic acid 2-Aminothiazole-4-acetic acid Glycine tert-Butanol Ethyl 2-(Chlorosulfonyl)acetate Cyclobutanecarboxylic acid DL-tert-Leucine 4-Hydroxy-D-(-)-2-phenylglycine BOC-Glycine Iminodiacetic acid