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ChemicalBook CAS DataBase List BOC-MET-MET-OH

BOC-MET-MET-OH synthesis

4synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: conc. H2SO4 / 3 h / Heating
2: 1.) chloroisobutyl formate, 2.) Et3N / 1.) dioxane, 0 deg C, 2.) dioxane, room temperature, overnight
3: 1 N NaOH / ethanol

References:

Kasai, Takanori;Tanaka, Tomoyuki;Kiriyama, Shuhachi [Bioscience, Biotechnology and Biochemistry,1996,vol. 60,# 5,p. 828 - 834]

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