ChemicalBook CAS DataBase List Borazine, hexamethyl-

Borazine, hexamethyl- synthesis

5synthesis methods

Product Name:Borazine, hexamethyl-
CAS Number:877-07-6
Molecular formula:C6H18B3N3
Molecular Weight:164.66

Borazine, 2,4,6-trichloro-1,3,5-trimethyl-

703-86-6
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75-16-1
269 suppliers
$12.00/10ml

1826-67-1
209 suppliers
$60.89/100ml

Borazine, 2-ethenyl-1,3,4,5,6-pentamethyl-

16898-38-7
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Borazine, 2,4-diethenyl-1,3,5,6-tetramethyl-

38828-96-5
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877-07-6
4 suppliers
$156.00/250MG

Yield:16898-38-7 63% ，38828-96-5 7% ，877-07-6 16%

Reaction Conditions:

in diethyl ether;N2 atmosphere; addn. of soln. of MeMgBr in Et2O to soln. of B-compd. in Et2O(room temp.), stirring (1 h, room temp.), addn. of vinylmagnesium bromide, stirring (overnight, room temp.); removal of solvent, extn. (hot hexane), removal of solvent, decompn. on futher purification;

References:

Jackson, Logan A.;Allen, Christopher W. [Journal of the Chemical Society, Dalton Transactions,1989,p. 2423 - 2428]

703-86-6
0 suppliers
inquiry

75-16-1
269 suppliers
$12.00/10ml

877-07-6
4 suppliers
$156.00/250MG

References