BORONIC ACID, B-(2,3-DIMETHOXY-4-PYRIDINYL)- synthesis
- Product Name:BORONIC ACID, B-(2,3-DIMETHOXY-4-PYRIDINYL)-
- CAS Number:1031438-93-3
- Molecular formula:C7H10BNO4
- Molecular Weight:182.97
52605-97-7
182 suppliers
$6.00/250mg
1031438-93-3
43 suppliers
$60.00/25mg
Yield:1031438-93-3 60%
Reaction Conditions:
Stage #1: 2,3-dimethoxypyridinewith n-butyllithium in tetrahydrofuran;hexane at 0; for 1 h;
Stage #2: with Triisopropyl borate in tetrahydrofuran;hexane at -78; for 2 h;
Stage #3: with acetic acid in water; pH=4;
References:
Smith, Amy E.;Clapham, Kate M.;Batsanov, Andrei S.;Bryce, Martin R.;Tarbit, Brian [European Journal of Organic Chemistry,2008,# 8,p. 1458 - 1463] Location in patent:experimental part