ChemicalBook CAS DataBase List Bromocyclopentane

Bromocyclopentane synthesis

12synthesis methods

Product Name:Bromocyclopentane
CAS Number:137-43-9
Molecular formula:C5H9Br
Molecular Weight:149.03

Bromocyclopentane is synthesized by bromination of cyclopentanol: cyclopentanol is mixed with hydrobromic acid and heated to about 170°C refluxed for 6-8h. Then distilled with water steam, the oil layer is washed with 5% sodium carbonate, then dried, filtered, fractionated and collected 136-139°C fraction is the finished product. Another method is by the reaction of cyclopentanol and phosphorus tribromide: the cyclopentanol is cooled to 0 ℃, add the newly evaporated phosphorus tribromide drop by drop, add it all at 0-5 ℃, stir for 2h, and leave it at room temperature overnight. Add water and stratify, take the oil layer water distillation. Distillate stratification, the oil layer was washed with 10% sodium bicarbonate solution, dried with anhydrous calcium chloride, filtration, filtrate distillation, collect 134-141 ℃ fraction that is bromocyclopentane.

287-92-3
304 suppliers
$22.00/25mL

137-43-9
314 suppliers
$13.00/25g

Yield:137-43-9 100%

Reaction Conditions:

with bromine;aluminium trichloride;Acetyl bromide in pentane at 0; for 1.83333 h;

References:

Akhrem, I. S.;Orlinkov, A. V.;Vitt, S. V.;Afanas'eva, L. V.;Vol'pin, M. E. [Bulletin of the Academy of Sciences of the USSR Division of Chemical Science,1989,vol. 38,# 91,p. 1864 - 1868][Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya,1989,# 9,p. 2028 - 2033]

96-41-3
253 suppliers
$10.00/10g

137-43-9
314 suppliers
$13.00/25g

References

5614-37-9
248 suppliers
$15.00/100mL

137-43-9
314 suppliers
$13.00/25g

References

287-92-3
304 suppliers
$22.00/25mL

137-43-9
314 suppliers
$13.00/25g

96-41-3
253 suppliers
$10.00/10g

References

1556-18-9 Synthesis

1556-18-9
91 suppliers
$38.96/5g

137-43-9
314 suppliers
$13.00/25g

References

Bromocyclopentane Related Search:

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