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BUTTPARK 144\07-81 synthesis

1synthesis methods
20776-50-5 Synthesis
2-Amino-4-bromobenzoic acid

20776-50-5
313 suppliers
$10.00/1g

BUTTPARK 144\07-81

573681-17-1
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Yield:573681-17-1 75%

Reaction Conditions:

Stage #1: chloroacetonitrilewith sodium in methanol at 25; for 0.666667 h;Inert atmosphere;
Stage #2: 2-amino-4-bromobenzoic acid in methanol at 25; for 2 h;Inert atmosphere;

References:

Li, Hong-Ze;He, Hai-Yun;Han, Yuan-Yuan;Gu, Xin;He, Lin;Qi, Qing-Rong;Zhao, Ying-Lan;Yang, Li [Molecules,2010,vol. 15,# 12,p. 9473 - 9485] Location in patent:experimental part

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