BUTYL TERT-BUTYL SULFIDE synthesis

4synthesis methods

Product Name:BUTYL TERT-BUTYL SULFIDE
CAS Number:926-47-6
Molecular formula:C8H18S
Molecular Weight:146.29

109-79-5
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75-65-0 Synthesis

75-65-0
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926-47-6
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$28.60/250mg

Yield:926-47-6 85%

Reaction Conditions:

with perchloric acid;acetic anhydride;acetic acid in water monomer at 0 - 20; for 12 h;

Steps:

8. Preparation of Substrates

General procedure: 8.5 Preparation of 3g, 3v. Thiophenol (4.0 mmol, 1.0 equiv.) was added to the mixture of glacial acetic acid (799.9 mg, 13.3 mmol,3.3 equiv.), 70% perchloric acid (562.5 mg, 5.6 mmol, 1.4 equiv.), and acetic anhydride (518.6 mg, 5.1 mmol,1.3 equiv.) at 0 °C. After tert-butanol (355.8 mg, 4.8 mmol, 1.2 equiv.) was added, the mixture was stirred atroom temperature for 12 h. Then, water (10 mL) was added to the mixture and extracted the reaction mixturewith EtOAc (8 mL × 3). The combined organic layers were washed with 20% aqueous sodium hydroxidesolution (10 mL × 2), dried with Na2SO4 and concentrated in vacuo to give the corresponding product.

References:

Li, Xiaotong;Wang, Yu;Xie, Xiaomin;Yang, Liqun;Zhang, Zhaoguo [Tetrahedron,2022,vol. 110,art. no. 132708] Location in patent:supporting information

507-19-7
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$10.00/5g

109-79-5
228 suppliers
$14.00/25g

926-47-6
3 suppliers
$28.60/250mg

References

Butane, 1-[(1,1-dimethylethyl)sulfinyl]-

13153-04-3
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926-47-6
3 suppliers
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References

109-65-9 Synthesis

109-65-9
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$10.00/10g

75-66-1
139 suppliers
$18.00/25mL

926-47-6
3 suppliers
$28.60/250mg

References