ChemicalBook CAS DataBase List C 1311

C 1311 synthesis

5synthesis methods

Product Name:C 1311
CAS Number:138154-39-9
Molecular formula:C20H22N4O2
Molecular Weight:350.41

55775-97-8 Synthesis

55775-97-8
108 suppliers
$7.00/100mg

138154-39-9
14 suppliers
$159.00/5mg

Yield:-

Steps:

Multi-step reaction with 5 steps
1.1: N,N-dimethyl-aniline / Inert atmosphere
2.1: trichlorophosphate / 1,2-dichloro-ethane / 90 °C
3.1: N,N-dimethyl-formamide / 4 h / Reflux
4.1: hydrazine hydrate / tetrahydrofuran / 24 h / 20 °C
4.2: 0.5 h / pH 3
5.1: 24 h / Reflux

References:

Dunstan, Mark S.;Barnes, John;Humphries, Matthew;Whitehead, Roger C.;Bryce, Richard A.;Leys, David;Stratford, Ian J.;Nolan, Karen A. [Journal of Medicinal Chemistry,2011,vol. 54,# 19,p. 6597 - 6611]

99009-49-1 Synthesis