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30860-31-2

CARBON DISULFIDE (13C) synthesis

2synthesis methods
-

Yield:30860-31-2 88%

Reaction Conditions:

in gaseous matrix;solid matrix;byproducts: iodine; CH3I/N2 mixture poured over a mixture of see sand and P4S10 (speed of the gas stream: 15 ml*min**-1) for 5 h, 330°C; iodine removed with KOH, gas stream cooled (trap cooled to -70°C), refreezed under vacuum, content of CS2: 99%;

References:

Abram, Ulrich;Kirmse, Reinhard;Bubner, Marianne [Zeitschrift fur Chemie,1982,vol. 22,p. 216 - 217]