CARBON DISULFIDE (13C) synthesis

2synthesis methods

Product Name:CARBON DISULFIDE (13C)
CAS Number:30860-31-2
Molecular formula:CS2
Molecular Weight:77.15

2,4,6,8,9,10-Hexathia-1,3,5,7-tetraphosphatricyclo[3.3.1.13,7]decane, 1,3,5,7-tetrasulfide

15857-57-5
0 suppliers
inquiry

4227-95-6
36 suppliers
$139.00/1g

30860-31-2
18 suppliers
$470.00/100mg

Yield:30860-31-2 88%

Reaction Conditions:

in gaseous matrix;solid matrix;byproducts: iodine; CH3I/N2 mixture poured over a mixture of see sand and P4S10 (speed of the gas stream: 15 ml*min**-1) for 5 h, 330°C; iodine removed with KOH, gas stream cooled (trap cooled to -70°C), refreezed under vacuum, content of CS2: 99%;

References:

Abram, Ulrich;Kirmse, Reinhard;Bubner, Marianne [Zeitschrift fur Chemie,1982,vol. 22,p. 216 - 217]

18555-26-5
0 suppliers
inquiry

75-15-0
253 suppliers
$40.00/100g

865-36-1
3 suppliers
inquiry

30860-31-2
18 suppliers
$470.00/100mg

References