CHEMBRDG-BB 4016764 synthesis

Yield:915925-11-0 96%

Reaction Conditions:

with lithium aluminium tetrahydride in tetrahydrofuran at 0 - 20; for 24.5 h;Inert atmosphere;Reflux;

References:

Atobe, Masakazu;Blakemore, David C.;Bond, Paul S.;Chan, Ngai S.;De Fusco, Claudia;Downes, Thomas D.;Firth, James D.;Hubbard, Roderick E.;Jones, S. Paul;Klein, Hanna F.;O'Brien, Peter;Roughley, Stephen D.;Vidler, Lewis R.;Waddelove, Laura;Whatton, Maria Ann;Wheldon, Mary C.;Woolford, Alison J.-A.;Wrigley, Gail L. [Chemistry - A European Journal,2020] Location in patent:supporting information