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ChemicalBook CAS DataBase List CHEMBRDG-BB 9070773
86926-54-7

CHEMBRDG-BB 9070773 synthesis

7synthesis methods
-

Yield:86926-54-7 84%

Reaction Conditions:

Stage #1: N-(4-methylbenzylidene)prop-2-en-1-aminewith C21H39NPPd(1-)*C2F3O2(1-);phenylsilane in chloroform-d1 at 40; for 4 h;Glovebox;Sealed tube;
Stage #2: with water in chloroform-d1;Sealed tube;Glovebox;regioselective reaction;

References:

Tafazolian, Hosein;Schmidt, Joseph A.R. [Catalysis science and technology,2016,vol. 6,# 3,p. 685 - 689]