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ChemicalBook CAS DataBase List CHLOROMETHYLTRIMETHYLTIN
4554-90-9

CHLOROMETHYLTRIMETHYLTIN synthesis

4synthesis methods
-

Yield:4554-90-9 80.6%

Reaction Conditions:

with CH3MgBr in diethyl ether;refluxing;;

References:

Khrapov, V. V.;Goldanskii, V. I.;Prokofev, A. K.;Kostyanovskii, R. G. [Zhurnal Obshchei Khimii,1967,vol. 37,p. 1 - 7][Zhurnal Obshchei Khimii,1967,vol. 37,p. 3 - 11] Kostyanovskii, R. G.;Prokofev, A. K. [Doklady Akademii nauk SSSR,1965,vol. 160/165,p. 969 - 972][Doklady Akademii Nauk SSSR,1965,vol. 164,p. 1054 - 1057] [Gmelin Handbuch der Anorganischen Chemie,Gmelin Handbook: Sn: Org.Verb.2, 1.1.2.1, page 6 - 20]