CHOLINE BIS(TRIFLUOROMETHYLSULFONYL)IMIDE synthesis

5synthesis methods

Product Name:CHOLINE BIS(TRIFLUOROMETHYLSULFONYL)IMIDE
CAS Number:827027-25-8
Molecular formula:C7H14F6N2O5S2
Molecular Weight:384.3169

67-48-1 Synthesis

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Lithium bis(trifluoromethanesulphonyl)imide

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CHOLINE BIS(TRIFLUOROMETHYLSULFONYL)IMIDE

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Yield:827027-25-8 100%

Reaction Conditions:

in water at 20; for 12 h;

Steps:

3.2.1. Synthesis of IL 1

To a solution of choline chloride (2 g, 14.39 mmol) in deionized water (2 mL) wasadded LiNTf2 (4.57 g, 15.83 mmol). The solution was stirred and allowed to undergo ionexchange at room temperature for 12 h. After this time, the mixture solution was extractedthree times with CH2Cl2. The combined organic layers were dried with anhydrous sodiumsulfate, filtered, and concentrated to afford colorless ionic liquid IL 1, [choline][NTf2] (5.53g, 100% yield) [6].

References:

Chen, Chien-Yuan;Chen, Jin-Syuan;Chu, Yen-Ho [Molecules,2022,vol. 27,# 1,art. no. 257]

90076-65-6
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$6.00/5g

827027-25-8
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inquiry

References