Chrysin 6-C-glucoside synthesis
2synthesis methods
- Product Name:Chrysin 6-C-glucoside
- CAS Number:28368-57-2
- Molecular formula:C21H20O9
- Molecular Weight:416.38
Yield:-
Steps:
Multi-step reaction with 4 steps
1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / Reflux
2: potassium hydroxide / pyridine / 1 h / 85 °C / Inert atmosphere
3: hydrogen; palladium 10% on activated carbon / methanol; tetrahydrofuran
4: recombinant Oryza sativa C-glycosyltransferase / ethanol / 30 °C / pH 7.5 / Enzymatic reaction
References:
Hao;Caulfield;Hamilton;Pickett;Midega;Khan;Wang;Hooper [Phytochemistry,2016,vol. 125,p. 73 - 87]
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