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ChemicalBook CAS DataBase List CIS-STYRENE-BETA-D

CIS-STYRENE-BETA-D synthesis

7synthesis methods
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Yield:21370-59-2 90%

Reaction Conditions:

Stage #1: Phenylacetylene-d1with Schwartz's reagent in dichloromethane at 0 - 20; for 2 h;Darkness;Inert atmosphere;
Stage #2: with water in dichloromethane at 20; for 2 h;Inert atmosphere;

References:

Berhal, Farouk;Grimaud, Laurence;Kirby, Georgina;Prestat, Guillaume;Vitale, Maxime R. [Green Chemistry,2021,vol. 23,# 23,p. 9428 - 9432] Location in patent:supporting information

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