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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide

Confertin synthesis

1synthesis methods
Azuleno[6,5-b]furan-2(3H)-one, decahydro-5-hydroxy-4a,8-dimethyl-3-methylene-, [3aR-(3aα,4aβ,5β,7aα,8β,9aα)]- (9CI)

114579-31-6
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Confertin

19908-69-1
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-

Yield:19908-69-1 84%

Reaction Conditions:

with pyridine;chromium(VI) oxide in dichloromethane; for 0.5 h;Ambient temperature;

References:

Quinkert, Gerhard;Schmalz, Hans-Guenther;Walzer, Egon;Gross, Stefan;Kowalczyk-Przewloka, Teresa;et al. [Liebigs Annalen der Chemie,1988,p. 283 - 316]