![](/CAS/20180808/GIF/116408-80-1.gif)
coriandrin synthesis
- Product Name:coriandrin
- CAS Number:116408-80-1
- Molecular formula:C13H10O4
- Molecular Weight:230.22
![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
1000210-73-0
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Yield:-
Steps:
Multi-step reaction with 6 steps
1: 100 percent / AcOK / 12 h / 120 °C
2: NBS, benzoyl peroxide / CCl4 / 16 h / 120 °C
3: 87 percent / PhCH2Pd(PPh3)2Cl / hexamethylphosphoric acid triamide / 6 h / 65 °C
4: 75 percent / LiOH / methanol; tetrahydrofuran; H2O / 40 h / 70 °C
5: 69 percent / Na2CO3, Pd(CH3CN)2Cl2 / tetrahydrofuran / 4 h / Ambient temperature
6: 89 percent / DEAD, Ph3P / 6 h / Ambient temperature
References:
Kraus, George A.;Ridgeway, James [Journal of Organic Chemistry,1994,vol. 59,# 17,p. 4735 - 4737]
![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
1000210-73-0
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![coriandrin](/CAS/20180808/GIF/116408-80-1.gif)
116408-80-1
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![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
1000210-73-0
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![coriandrin](/CAS/20180808/GIF/116408-80-1.gif)
116408-80-1
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![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
1000210-73-0
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![coriandrin](/CAS/20180808/GIF/116408-80-1.gif)
116408-80-1
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