CYANOMETHYLENETRIBUTYLPHOSPHORANE synthesis
- Product Name:CYANOMETHYLENETRIBUTYLPHOSPHORANE
- CAS Number:157141-27-0
- Molecular formula:C14H28NP
- Molecular Weight:241.35
998-40-3
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$18.32/25g
157141-27-0
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$16.00/1g
Yield:-
Steps:
Multi-step reaction with 2 steps
1: 91 percent / nitromethane / 16 h / 20 °C
2: 95 percent / n-butyllithium / hexane / 20 h / 0 - 20 °C
References:
Sakamoto, Izumi;Nishii, Takeshi;Ozaki, Fumie;Kaku, Hiroto;Tanaka, Masami;Tsunoda, Tetsuto [Chemical and Pharmaceutical Bulletin,2005,vol. 53,# 11,p. 1508 - 1509]