Cyclohexene, 1-(2-nitro-2-propen-1-yl)- synthesis
2synthesis methods
- Product Name:Cyclohexene, 1-(2-nitro-2-propen-1-yl)-
- CAS Number:80255-20-5
- Molecular formula:C9H13NO2
- Molecular Weight:167.21
Yield:80255-20-5 50.4%
Reaction Conditions:
with n-butyllithium in tetrahydrofuran;diethyl ether;1.) -78 deg C, -60 deg C, 0.5 h , 2.) -100 deg C,in ether, 1.5 h, -80 deg C, -30 deg C in 10 min;
References:
Seebach, Dieter;Knocherl, Paul [Helvetica Chimica Acta,1984,vol. <1> 67,# 32,p. 261 - 283]
