Cyclopent-3-enecarboxylic acid benzylamide synthesis
- Product Name:Cyclopent-3-enecarboxylic acid benzylamide
- CAS Number:40810-36-4
- Molecular formula:C13H15NO
- Molecular Weight:201.26
Yield:40810-36-4 684mg
Reaction Conditions:
Stage #1: 3-cyclopentene-1-carboxylic acidwith oxalyl dichloride in dichloromethane;N,N-dimethyl-formamide at 0 - 20; for 1.5 h;Inert atmosphere;
Stage #2: benzylaminewith triethylamine in dichloromethane;N,N-dimethyl-formamide at 0 - 20;Inert atmosphere;
References:
Hoang, Gia L.;Yang, Zhao-Di;Smith, Sean M.;Miska, Judy L.;Prez, Damaris E.;Zeng, Xiao Cheng;Takacs, James M.;Pal, Rhitankar;Pelter, Libbie S. W. [Organic Letters,2015,vol. 17,# 4,p. 940 - 943] Location in patent:supporting information
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