Cyclopenta[b]thiopyran synthesis
- Product Name:Cyclopenta[b]thiopyran
- CAS Number:271-17-0
- Molecular formula:C8H6S
- Molecular Weight:134.2
![Cyclopenta[b]thiopyran-3-ol, 2,3,4,5,6,7-hexahydro-](/CAS/20210305/GIF/90198-90-6.gif)
90198-90-6
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271-17-0
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Yield:-
Steps:
Multi-step reaction with 2 steps
1: 1.) NaH / 1.) DMF, a) 25 deg C, 12 h, b) from 25 deg C, to 75 deg C, 5 min, 2.) DMF, 12 h
2: 2.) Pd/C/MgO / 1.) 110 deg C, 2.) 370 deg C
References:
Klein, Robert F. X.;Horak, Vaclav [Journal of Organic Chemistry,1986,vol. 51,# 24,p. 4644 - 4651]
![Carbamothioic acid, N,N-dimethyl-, O-(2,3,4,5,6,7-hexahydrocyclopenta[b]thiopyran-3-yl) ester](/CAS/20210305/GIF/104576-71-8.gif)
104576-71-8
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271-17-0
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![Cyclopentanone, 2-[(2-oxopropyl)thio]-](/CAS/20210305/GIF/104576-69-4.gif)
104576-69-4
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271-17-0
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