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β-cyclopentylethyl bromide synthesis

10synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: H2 / 5percent Pd/C / ethanol / 760 Torr
2: LiAlH4 / tetrahydrofuran
3: PBr3 / diethyl ether; diethyl ether / 16 h / Ambient temperature

References:

Yokohama;Miwa;Aibara;Fujiwara;Matsumoto;Nakayama;Iwamoto;Mori;Moroi;Tsukada;Isoda [Chemical and Pharmaceutical Bulletin,1992,vol. 40,# 9,p. 2391 - 2398]

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