D-2-THIENYLALANINE synthesis
- Product Name:D-2-THIENYLALANINE
- CAS Number:62561-76-6
- Molecular formula:C7H9NO2S
- Molecular Weight:171.22
636-72-6
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62561-76-6
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Yield:-
Steps:
Multi-step reaction with 6 steps
1.1: SOCl2; benzotriazole / CH2Cl2
2.1: NaH / dimethylformamide; various solvent(s) / 0.5 h / 20 °C
2.2: 82 percent / dimethylformamide; various solvent(s) / 7 h / 20 - 60 °C
3.1: NaOH / methanol / 20 h / 20 °C
4.1: toluene / 2 h / Heating
5.1: 75 percent / aq. LiOH / 2.5 h / 60 °C
6.1: 45 percent / phenylalanine ammonia-lyase / various solvent(s) / 48 h / 30 °C / pH 8.8
References:
Paizs, Csaba;Katona, Adrian;Retey, Janos [Chemistry - A European Journal,2006,vol. 12,# 10,p. 2739 - 2744]
2021-58-1
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62561-76-6
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2021-58-1
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73495-10-0
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62561-76-6
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98-03-3
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62561-76-6
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![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
1000210-73-0
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62561-76-6
127 suppliers
$17.00/250mg