D-Glutamic acid, 1,5-bis(1,1-dimethylethyl) ester synthesis

7synthesis methods

Product Name:D-Glutamic acid, 1,5-bis(1,1-dimethylethyl) ester
CAS Number:92837-84-8
Molecular formula:C13H25NO4
Molecular Weight:259.34

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D-Glutamic acid, 1,5-bis(1,1-dimethylethyl) ester

92837-84-8
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: boron trifluoride diethyl etherate / dichloromethane; cyclohexane / 20 °C
2: acetic acid; hydrogenchloride / ethyl acetate / 2 h / 20 °C / Cooling with ice

References:

Guzelj, Samo;Nabergoj, Sanja;Gobec, Martina;Pajk, Stane;Klančič, Veronika;Slütter, Bram;Frkanec, Ruža;Štimac, Adela;Šket, Primož;Plavec, Janez;Mlinarič-Raščan, Irena;Jakopin, Žiga [Journal of Medicinal Chemistry,2021,vol. 64,# 11,p. 7809 - 7838]