![](/CAS/GIF/160557-06-2.gif)
D-Norleucine, 2-(aminomethyl)- (9CI) synthesis
- Product Name:D-Norleucine, 2-(aminomethyl)- (9CI)
- CAS Number:160557-06-2
- Molecular formula:C7H16N2O2
- Molecular Weight:160.21
![D-Norleucine](/CAS/GIF/327-56-0.gif)
327-56-0
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![D-Norleucine, 2-(aminomethyl)- (9CI)](/CAS/GIF/160557-06-2.gif)
160557-06-2
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Yield:-
Steps:
Multi-step reaction with 4 steps
1: 95 percent / 1 M aq. NaOH / ethanol
2: 56 percent / CH2Cl2 / -20 °C
3: 1.) LiN(SiMe3)2 / 1.) THF, from -78 to -65 deg C, 2.) THF
4: 86 percent / 40percent w/v aq. HBr / 3 h / Heating
References:
Jones, Raymond C. F.;Crockett, Alan K.;Rees, David C.;Gilbert, Ian H. [Tetrahedron Asymmetry,1994,vol. 5,# 9,p. 1661 - 1664]