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Daniquidone synthesis

5synthesis methods
Carbamic acid, [4-(acetylamino)-2-[(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)methyl]phenyl]-, ethyl ester (9CI)

129276-20-6
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Daniquidone

67199-66-0
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Yield:67199-66-0 95%

Reaction Conditions:

with sulfuric acid at 100; for 5 h;

References:

Rosevear, Judi;Wilshire, John F. K. [Australian Journal of Chemistry,1990,vol. 43,# 2,p. 339 - 353]