decyl benzoate synthesis
15synthesis methods
- Product Name:decyl benzoate
- CAS Number:36685-97-9
- Molecular formula:C17H26O2
- Molecular Weight:262.39
Decyl benzoate is produced by direct esterification of n-Decanol with Benzoic acid under azeotropic conditions.
Yield:36685-97-9 97%
Reaction Conditions:
Stage #1: 1-Decanol;N,N-diethyl-α,α-difluorobenzylamine in dichloromethane at 0; for 0.5 h;Inert atmosphere;
Stage #2: with water;sodium hydrogencarbonate in dichloromethane;Saturated solution;
References:
Wakita, Natsumi;Hara, Shoji [Tetrahedron,2010,vol. 66,# 40,p. 7939 - 7945] Location in patent:experimental part