deoxythymidylyl-3'-5'-deoxyadenylate synthesis

2synthesis methods

Product Name:deoxythymidylyl-3'-5'-deoxyadenylate
CAS Number:2147-15-1
Molecular formula:C20H27N7O13P2
Molecular Weight:635.41

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Yield:-

Steps:

Multi-step reaction with 2 steps
1: 79 percent / Ph₃P, 2,2'-dipyridyl disulfide / pyridine / 24 h / Ambient temperature
2: 1.) benzoic anhydride, AgOAc, 2.) isoamyl nitrite, 3.) H₂S / 1.) pyridine-AcOH, r.t.; 2.) pyridine, AcOH, r.t., 6 h; 3.) pyridine-AcOH, r.t.

References:

Nishizawa, Makoto;Kurihara, Takashi;Hata, Tsujiaki [Chemistry Letters,1984,p. 175 - 178]

5'-Adenylic acid, N-benzoyl-2'-deoxy- (9CI)

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References