![](/CAS/GIF/28610-31-3.gif)
Desmethylanhydroicaritin synthesis
- Product Name:Desmethylanhydroicaritin
- CAS Number:28610-31-3
- Molecular formula:C20H18O6
- Molecular Weight:354.35
![2',4',6'-Trihydroxyacetophenone monohydrate](/CAS/GIF/480-66-0.gif)
480-66-0
345 suppliers
$10.00/1g
![Desmethylanhydroicaritin](/CAS/GIF/28610-31-3.gif)
28610-31-3
58 suppliers
$125.00/1 mg
Yield:-
Steps:
Multi-step reaction with 9 steps
1.1: potassium carbonate / acetone / 20 °C
2.1: potassium hydroxide / ethanol / 48 h / 20 °C
3.1: iodine / dimethyl sulfoxide / 24 h / Reflux
4.1: Oxone; sodium carbonate; sodium hydrogencarbonate / dichloromethane; acetone / 5 h / 0 °C
4.2: 0.5 h / 20 °C
5.1: hydrogenchloride / ethanol; water / 0.5 h / 20 °C
6.1: potassium carbonate / acetone / 0.5 h / 20 °C
6.2: 2 h / 20 °C
7.1: potassium carbonate / acetone / 1 h / 20 °C
7.2: 5 h / 50 °C
8.1: N,N-diethylaniline / 0.75 h / 190 °C / Microwave irradiation; Inert atmosphere
9.1: hydrogenchloride / water; methanol / 2 h / Reflux
References:
Nguyen, Van-Son;Dong, Lin-Pei;Wang, Sheng-Chun;Wang, Qiuan [European Journal of Organic Chemistry,2015,vol. 2015,# 10,p. 2297 - 2302]
![Icaritin](/CAS/GIF/118525-40-9.gif)
118525-40-9
207 suppliers
$5.00/5mg
![Desmethylanhydroicaritin](/CAS/GIF/28610-31-3.gif)
28610-31-3
58 suppliers
$125.00/1 mg
![DesMethyl Icaritin Tri-O-MethoxyMethyl Ether](/CAS/GIF/143724-76-9.gif)
143724-76-9
7 suppliers
$55.00/1mg
![Desmethylanhydroicaritin](/CAS/GIF/28610-31-3.gif)
28610-31-3
58 suppliers
$125.00/1 mg
![KaeMpferol Tri-O-MethoxyMethyl Ether](/CAS/20180808/GIF/143724-66-7.gif)
143724-66-7
9 suppliers
inquiry
![Desmethylanhydroicaritin](/CAS/GIF/28610-31-3.gif)
28610-31-3
58 suppliers
$125.00/1 mg
![5-O-(3-Methyl-2-butenyl) KaeMpferol Tri-O-MethoxyMethyl Ether](/CAS/GIF/143724-70-3.gif)
143724-70-3
10 suppliers
$80.00/2mg
![Desmethylanhydroicaritin](/CAS/GIF/28610-31-3.gif)
28610-31-3
58 suppliers
$125.00/1 mg