![](/CAS/GIF/625-22-9.gif)
DI-N-BUTYL SULFATE synthesis
- Product Name:DI-N-BUTYL SULFATE
- CAS Number:625-22-9
- Molecular formula:C8H18O4S
- Molecular Weight:210.29
![Tributyl borate](/CAS/GIF/688-74-4.gif)
688-74-4
320 suppliers
$10.40/25mL
![DI-N-BUTYL SULFATE](/CAS/GIF/625-22-9.gif)
625-22-9
69 suppliers
$15.00/5g
Yield:-
Reaction Conditions:
with sulfuric acid at 90;Cooling with ice;
Steps:
1 Example 1
While tributyl borate in the reactor transferred into an ice-bathe is being stirred with amechanical mixer, 300 g H2SO4 is added dropwise. After the mixture is stirred in ice-bathe for 1-3 hours, and at roomtemperature for 2-3 hours, it is stirred at 60-90 °C for 24 hours. In order to eliminate the acid residues, the liquid mixtureis mixed with 50g commercial poly(4-vinyl pyridine) and filtered through a silica column (10cm). The light brown liquidproduct, dibutyl sulfate, is stored in a tightly sealed glass bottle.
References:
Ulusal Bor Arastirma Enstitusu;Bicak, Niyazi EP2851362, 2015, A1 Location in patent:Paragraph 0034
![dibutyl sulphite](/CAS/GIF/626-85-7.gif)
626-85-7
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inquiry
![DI-N-BUTYL SULFATE](/CAS/GIF/625-22-9.gif)
625-22-9
69 suppliers
$15.00/5g
![TRIBUTYL PHOSPHITE](/CAS/GIF/102-85-2.gif)
102-85-2
158 suppliers
$14.00/5mL
![DI-N-BUTYL SULFATE](/CAS/GIF/625-22-9.gif)
625-22-9
69 suppliers
$15.00/5g
![Tributyl phosphate](/CAS/GIF/126-73-8.gif)
126-73-8
525 suppliers
$6.00/100g
![Dibutyl butanephosphonate](/CAS/GIF/78-46-6.gif)
78-46-6
40 suppliers
$79.50/5ml-f
![TRIBUTYL PHOSPHITE](/CAS/GIF/102-85-2.gif)
102-85-2
158 suppliers
$14.00/5mL
![DI-N-BUTYL SULFATE](/CAS/GIF/625-22-9.gif)
625-22-9
69 suppliers
$15.00/5g
![Tributyl phosphate](/CAS/GIF/126-73-8.gif)
126-73-8
525 suppliers
$6.00/100g
![O,O,O-TRIBUTYL PHOSPHOROTHIOATE](/CAS/GIF/78-47-7.gif)
78-47-7
8 suppliers
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![Dibutyl butanephosphonate](/CAS/GIF/78-46-6.gif)
78-46-6
40 suppliers
$79.50/5ml-f
![Chlorosulfuric acid, butyl ester](/CAS/20180527/GIF/763-23-5.gif)
763-23-5
0 suppliers
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![DI-N-BUTYL SULFATE](/CAS/GIF/625-22-9.gif)
625-22-9
69 suppliers
$15.00/5g