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ChemicalBook CAS DataBase List DI-N-BUTYLTIN SULFIDE

DI-N-BUTYLTIN SULFIDE synthesis

13synthesis methods
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Yield: 91%

Reaction Conditions:

with carbon disulfide;tributylphosphine in 1,2-dichloro-ethaneunder N2; CS2 was added to a soln. of the Sn-compound and Bu3P; stirred for 5 h at 50°C; excess CS2 and solvent were removed in vac.; column chromy. (silica gel; eluent: C6H6); elem. anal.; NMR; IR;

References:

Yano, Katsunori;Baba, Akio;Matsuda, Haruo [Chemische Berichte,1991,vol. 124,# 8,p. 1881 - 1884]