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ChemicalBook CAS DataBase List DI-T-BUTYLMETHYLSILANE

DI-T-BUTYLMETHYLSILANE synthesis

3synthesis methods
-

Yield:56310-20-4 86%

Reaction Conditions:

Stage #1: Dichloromethylsilane;tert.-butyl lithium in pentane at 0;Inert atmosphere;Schlenk technique;
Stage #2: at 20; for 48 h;

References:

Basford, Annabel R.;Berryman, Victoria E. J.;Kaltsoyannis, Nikolas;Liddle, Stephen T.;Mills, David P.;Nodaraki, Lydia E.;Réant, Benjamin L. L.;Tuna, Floriana;Wooles, Ashley J. [Journal of the American Chemical Society,2021,vol. 143,# 26,p. 9813 - 9824] Location in patent:supporting information

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