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ChemicalBook CAS DataBase List DIALLYLDIBROMOTIN

DIALLYLDIBROMOTIN synthesis

3synthesis methods
-

Yield:17381-88-3 85%

Reaction Conditions:

with catalyst: 15-crown-5 in neat (no solvent);addn. of allyl bromide to stirred mixt. of Sn and 15-crown-5 (90-100°C, N2 stream); evapn. in N2 stream (80-100 Torr, 40°C), fractionation; elem. anal.;

References:

Kotlyar, S. A.;Dimitrishchuk, G. V.;Savranskaya, R. L.;Luk'yanenko, N. G. [Journal of general chemistry of the USSR,1988,vol. 58,p. 1287 - 1287][J.Gen.Chem.USSR (Engl.Transl.),1988,vol. 58,p. 1443 - 1443]