![](/CAS/GIF/1531-77-7.gif)
Dibenzo[b,e]thiepin-11(6H)-one synthesis
- Product Name:Dibenzo[b,e]thiepin-11(6H)-one
- CAS Number:1531-77-7
- Molecular formula:C14H10OS
- Molecular Weight:226.29
![o-Toluic acid](/CAS/GIF/118-90-1.gif)
118-90-1
489 suppliers
$13.00/1g
![Dibenzo[b,e]thiepin-11(6H)-one](/CAS/GIF/1531-77-7.gif)
1531-77-7
157 suppliers
$17.00/5g
Yield:-
Steps:
Multi-step reaction with 5 steps
1: potassium carbonate / N,N-dimethyl-formamide / 20 °C
2: N-Bromosuccinimide / tetrachloromethane / Reflux
3: potassium carbonate / acetone / Reflux
4: sodium hydroxide / water; ethanol / 20 °C
5: polyphosphoric acid / 120 °C
References:
Akiyama, Toshiyuki;Hasegawa, Yasushi;Kawai, Makoto;Miyagawa, Masayoshi;Noshi, Takeshi;Shishido, Takao;Taoda, Yoshiyuki;Tomita, Kenji;Yoshida, Ryu [Bioorganic and Medicinal Chemistry Letters,2020,vol. 30,# 22,art. no. 127547]
![2-PHENYLTHIOMETHYLBENZOIC ACID](/CAS/GIF/1699-03-2.gif)
1699-03-2
44 suppliers
$70.00/100mg
![Dibenzo[b,e]thiepin-11(6H)-one](/CAS/GIF/1531-77-7.gif)
1531-77-7
157 suppliers
$17.00/5g
![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
1000210-73-0
0 suppliers
inquiry
![Dibenzo[b,e]thiepin-11(6H)-one](/CAS/GIF/1531-77-7.gif)
1531-77-7
157 suppliers
$17.00/5g
![Benzonitrile, 2-[(phenylthio)methyl]-](/CAS/20210305/GIF/92164-25-5.gif)
92164-25-5
0 suppliers
inquiry
![Dibenzo[b,e]thiepin-11(6H)-one](/CAS/GIF/1531-77-7.gif)
1531-77-7
157 suppliers
$17.00/5g
![Ethyl 2-methylbenzoate](/CAS/GIF/87-24-1.gif)
87-24-1
144 suppliers
$14.00/1g
![Dibenzo[b,e]thiepin-11(6H)-one](/CAS/GIF/1531-77-7.gif)
1531-77-7
157 suppliers
$17.00/5g