DIBENZYL DIMETHYL SILANE synthesis
- Product Name:DIBENZYL DIMETHYL SILANE
- CAS Number:17964-30-6
- Molecular formula:C16H20Si
- Molecular Weight:240.42
13029-09-9
284 suppliers
$20.00/1g
1833-31-4
99 suppliers
$60.00/100mg
13688-68-1
51 suppliers
$20.00/100mg
17964-30-6
13 suppliers
$28.60/50MG
Yield:13688-68-1 60% ，17964-30-6 22%
Reaction Conditions:
Stage #1: 2,2'-dibromobiphenylwith tert.-butyl lithium in tetrahydrofuran;pentane at -75 - -60; for 1 h;
Stage #2: benzyl(chloro)dimethylsilanewith triethylamine in tetrahydrofuran;pentane at 20; for 1.5 h;
References:
Hudrlik, Paul F.;Dai, Donghua;Hudrlik, Anne M. [Journal of Organometallic Chemistry,2006,vol. 691,# 6,p. 1257 - 1264]
1631-70-5
92 suppliers
$7.00/250mg
17964-30-6
13 suppliers
$28.60/50MG