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Dichloro(DPPE)digold(I) ,96% synthesis

5synthesis methods
-

Yield:18024-34-5 99%

Reaction Conditions:

in benzene;byproducts: CO; soln. of Ph2PCH2CH2PPh2 dropped to soln. of (OC)AuCl at room temp. under dry N2, stirred for 1 h (CO removed); filtered;

References:

Schmidbaur, Hubert;Inoguchi, Yoshio [Chemische Berichte,1980,vol. 113,# 5,p. 1646 - 1653]