DICHLOROETHOXYOXOVANADIUM (V) synthesis

4synthesis methods

Product Name:DICHLOROETHOXYOXOVANADIUM (V)
CAS Number:1801-77-0
Molecular formula:C2H5Cl2O2V
Molecular Weight:182.91

1825-62-3
183 suppliers
$22.00/25g

7727-18-6 Synthesis

7727-18-6
60 suppliers
$16.19/10g

1801-77-0
6 suppliers
inquiry

Yield:1801-77-0 97%

Reaction Conditions:

in dichloromethane;byproducts: (CH3)3SiCl; (N2); addn. of 2 equiv. of silane deriv. to CH2Cl2 soln. of vanadium compd. at room temp., stirring for 2 h at room temp.; evapn., elem. anal.;

References:

Romero-Fernandez, Javier;Carrillo-Hermosilla, Fernando;Antinolo, Antonio;Alonso-Moreno, Carlos;Rodriguez, Ana M.;Lopez-Solera, Isabel;Otero, Antonio [Dalton Transactions,2010,vol. 39,# 28,p. 6419 - 6425]

64-17-5 Synthesis