DICHLOROMETHYLDIISOPROPOXYBORANE synthesis
- Product Name:DICHLOROMETHYLDIISOPROPOXYBORANE
- CAS Number:62260-99-5
- Molecular formula:C7H15BCl2O2
- Molecular Weight:212.91
Yield:62260-99-5 84%
Reaction Conditions:
with hydrogenchloride in diethyl ether;under N2; to cold (-98 °C) soln. of boron compd. in Et2O slowly added Cl2HCLi, stirred for 1 h, warmed to room temp., stirred for 3 h, cooled to 0 °C, added soln. of anhyd. HCl in Et2O, stirred for 0.5 h; decanted and combined with ether washes of solid, evapd. in air, distd.; elem. anal.;
References:
Brown, Herbert C.;Cole, Thomas E. [Organometallics,1983,vol. 2,# 10,p. 1316 - 1319]
5419-55-6
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62260-99-5
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62260-99-5
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