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ChemicalBook CAS DataBase List diethyl 2,3-diisopropylsuccinate

diethyl 2,3-diisopropylsuccinate synthesis

7synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1.1: ethanol; potassium / 1 h / 20 °C / Inert atmosphere
1.2: 9 h / Inert atmosphere; Reflux
2.1: sulfuric acid / water / 16 h / 160 °C
2.2: 0.75 h / 50 °C
3.1: sulfuric acid / ethanol / 24 h / Reflux

References:

China Petroleum&Chemical Corporation;Beijing Research Institute of Chemical Industry, China Petroleum & Chemical Corporation EP2399902, 2011, A1

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