DIETHYL 4-OXOCYCLOHEXANE-1,1-DICARBOXYLATE synthesis
- Product Name:DIETHYL 4-OXOCYCLOHEXANE-1,1-DICARBOXYLATE
- CAS Number:55704-60-4
- Molecular formula:C12H18O5
- Molecular Weight:242.27
105-53-3
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55704-60-4
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Yield:-
Steps:
Multi-step reaction with 2 steps
1: potassium tert-butylate / tetrahydrofuran / 4 h / 10 - 35 °C / Inert atmosphere
2: water; sodium chloride / dimethyl sulfoxide / 3.5 h / 160 °C / Inert atmosphere
References:
BRISTOL-MYERS SQUIBB COMPANY;UEDA, Yasutsugu;CONNOLLY, Timothy P.;JOHNSON, Barry L.;LI, Chen;NAIDU, B. Narasimhulu;PATEL, Manoj;PEESE, Kevin;SORENSON, Margaret E.;WALKER, Michael A.;BOWSHER, Michael S.;LI, Rongti WO2012/78834, 2012, A1
92454-00-7
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57899-62-4
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6297-36-5
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1444-05-9
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55704-60-4
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