![](/CAS/GIF/628-39-7.gif)
DIETHYLDISELENIDE synthesis
- Product Name:DIETHYLDISELENIDE
- CAS Number:628-39-7
- Molecular formula:C4H10Se2
- Molecular Weight:216.04
![Iodoethane](/CAS/20180808/GIF/75-03-6.gif)
75-03-6
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$11.00/5g
![DIETHYLDISELENIDE](/CAS/GIF/628-39-7.gif)
628-39-7
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$100.00/5g
Yield:628-39-7 99%
Reaction Conditions:
with selenium;potassium hydroxide in water at 60; for 0.5 h;
Steps:
2 Example 2: Preparation of Dialkyl Diselenide Compound II-2
The reaction formula is as follows:Add 99mg (1.25mmol) of selenium powder and 84mg (1.5mmol) of potassium hydroxide to the reaction flask, then add 0.5mL of water, and then add 156mg of ethyl iodide (1mmol) I-2 into the reaction flask under stirring. The reaction was stopped for 0.5h at 60°C. Filter, wash the filter cake twice with ethyl acetate (1mL×2), combine the filtrates, add 3 mL of water, mix well and stand for separation. After collecting the ethyl acetate layer, the water layer is washed with ethyl acetate (2mL×2). ) Extract twice, combine the ethyl acetate phases, and evaporate the ethyl acetate on a rotary evaporator to obtain 107 mg of dialkyl diselenide compound II-2 with a yield of 99%.
References:
CN113666857,2021,A Location in patent:Paragraph 0037-0041
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74-96-4
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![DIETHYLDISELENIDE](/CAS/GIF/628-39-7.gif)
628-39-7
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![Acetaldehyde](/CAS/GIF/75-07-0.gif)
75-07-0
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$14.00/5mL
![DIETHYLDISELENIDE](/CAS/GIF/628-39-7.gif)
628-39-7
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$100.00/5g
![Bromoethane](/CAS/20180906/GIF/74-96-4.gif)
74-96-4
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$9.00/5g
![Diethyl disulfide](/CAS/GIF/110-81-6.gif)
110-81-6
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$45.00/25g
![DIETHYLDISELENIDE](/CAS/GIF/628-39-7.gif)
628-39-7
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$100.00/5g
![DIETHYL SELENIDE](/CAS/GIF/627-53-2.gif)
627-53-2
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![Ethanesulfenoselenoic acid, ethyl ester (9CI)](/CAS/20210305/GIF/88890-93-1.gif)
88890-93-1
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