DIETHYLSTILBESTROL DIMETHYL ETHER synthesis
- Product Name:DIETHYLSTILBESTROL DIMETHYL ETHER
- CAS Number:7773-34-4
- Molecular formula:C20H24O2
- Molecular Weight:296.4
121-97-1
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7773-34-4
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$106.00/1g
Yield:-
Steps:
Multi-step reaction with 4 steps
1: ZnI2 / 36 h / Ambient temperature
2: SnCl2*2H2O / HCl; acetic acid / Heating
3: n-BuLi, diisopropyl amine, I2 / tetrahydrofuran; hexane / 1.) room temperature, 1h, 2.) 4 h, 3.) -75 deg C, 16 h
4: Pb(OAc)4 / tetrahydrofuran / 72 h / Heating
References:
Belletire, J. L.;Conroy, G. M. [Synthetic Communications,1988,vol. 18,# 4,p. 403 - 416]