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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide

dihydroindeno-2',1':2,3-fluorene synthesis

12synthesis methods
1,1':3',1''-Terphenyl, 2,2''-dichloro-4',6'-dimethyl-

1263048-16-3
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dihydroindeno-2',1':2,3-fluorene

525-18-8
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Yield:525-18-8 91%

Reaction Conditions:

with N,N′-bis(2,6-diisopropylphenyl)imidazol-2-ylidene hydrochloride;palladium diacetate;potassium carbonate in 1-methyl-pyrrolidin-2-one at 170; for 2 h;Inert atmosphere;Sealed tube;

References:

Hsiao, Chien-Chi;Lin, Yi-Kuan;Liu, Chia-Ju;Wu, Tsun-Cheng;Wu, Yao-Ting [Advanced Synthesis and Catalysis,2010,vol. 352,# 18,p. 3267 - 3274] Location in patent:experimental part

Indeno[2,1-b]fluorene-10,12-dione

112865-17-5
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dihydroindeno-2',1':2,3-fluorene

525-18-8
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References
1,3-Dibromobenzene

108-36-1
446 suppliers
$10.00/1g

Diphenylacetylene

501-65-5
212 suppliers
$16.00/5g

dihydroindeno-2',1':2,3-fluorene

525-18-8
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References
269410-07-3 Synthesis
1,2-bis(4,4,5,5-tetramethyl-[1,3,2]dioxabororan-2-yl)benzene

269410-07-3
68 suppliers
$37.00/100mg

35510-03-3 Synthesis
1,5-DIBROMO-2,4-BIS-BROMOMETHYL-BENZENE

35510-03-3
47 suppliers
$172.00/25mg

dihydroindeno-2',1':2,3-fluorene

525-18-8
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References
615-87-2 Synthesis
1,5-Dibromo-2,4-dimethylbenzene

615-87-2
89 suppliers
$9.00/250mg

dihydroindeno-2',1':2,3-fluorene

525-18-8
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References