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525-18-8

dihydroindeno-2',1':2,3-fluorene synthesis

12synthesis methods
-

Yield:525-18-8 91%

Reaction Conditions:

with N,N′-bis(2,6-diisopropylphenyl)imidazol-2-ylidene hydrochloride;palladium diacetate;potassium carbonate in 1-methyl-pyrrolidin-2-one at 170; for 2 h;Inert atmosphere;Sealed tube;

References:

Hsiao, Chien-Chi;Lin, Yi-Kuan;Liu, Chia-Ju;Wu, Tsun-Cheng;Wu, Yao-Ting [Advanced Synthesis and Catalysis,2010,vol. 352,# 18,p. 3267 - 3274] Location in patent:experimental part