DIISOPROPYLCARBAMOYL CHLORIDE synthesis
- Product Name:DIISOPROPYLCARBAMOYL CHLORIDE
- CAS Number:19009-39-3
- Molecular formula:C7H14ClNO
- Molecular Weight:163.65
4136-91-8
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19009-39-3
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Yield: 88.65%
Reaction Conditions:
Stage #1:tetraisopropylothiuram disulphide with chlorine in dichloromethane at 24 - 26; for 7.16667 h;Cooling with ice;
Stage #2: with water;sodium hydrogencarbonate in dichloromethaneCooling with ice;
References:
Adeppa;Rupainwar;Misra, Krishna [Synthetic Communications,2011,vol. 41,# 2,p. 285 - 290] Location in patent:experimental part
32315-10-9
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108-18-9
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19009-39-3
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20652-39-5
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19009-39-3
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2700-30-3
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19009-39-3
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