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62263-67-6

(Diisopropylphosphino)(Diphenylphosphino)methane synthesis

2synthesis methods
-

Yield:62263-67-6 3.66 g

Reaction Conditions:

Stage #1: diphenyl(methyl)phosphinewith n-butyllithium;potassium tert-butylate in diethyl ether;
Stage #2: Chlorodiisopropylphosphane in tetrahydrofuran at -78;Further stages.;

References:

Izod, Keith;McFarlane, William;Tyson, Brent V. [European Journal of Organic Chemistry,2004,# 5,p. 1043 - 1048]