Dimethoxymethylphenylsilane synthesis
- Product Name:Dimethoxymethylphenylsilane
- CAS Number:3027-21-2
- Molecular formula:C9H14O2Si
- Molecular Weight:182.29
1185-55-3
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$6.00/25g
100-58-3
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$18.00/10ml
3027-21-2
275 suppliers
$8.00/5g
Yield:3027-21-2 95%
Reaction Conditions:
in diethyl ether; for 1 h;Reflux;
Steps:
3
5L four-necked flask by adding 240g methyltrimethoxysilane and 1000mL ether, stirring drop 1080mL 1.63mol / L bromobenzene reagent ether solution; drop Bi, heated reflux 1h .; cooling, to the reaction (Yield 95%) of phenylmethyldimethoxysilane and 4 g of diphenylmethoxysilane (yield 1%) were added to the filtrate by adding 1000 mL of n-hexane and then filtering.
References:
CN103113400,2016,B Location in patent:Paragraph 0051; 0052
1185-55-3
460 suppliers
$6.00/25g
108-90-7
645 suppliers
$10.00/25G
3027-21-2
275 suppliers
$8.00/5g
67-56-1
739 suppliers
$9.00/25ml
124-41-4
682 suppliers
$12.00/25g
149-74-6
167 suppliers
$14.14/5gm:
3027-21-2
275 suppliers
$8.00/5g
67-56-1
739 suppliers
$9.00/25ml
149-74-6
167 suppliers
$14.14/5gm:
3027-21-2
275 suppliers
$8.00/5g
